Publication Date: 6/1/76
    Pages: 8
    Date Entered: 1/5/93
    Title: Shipping and Receiving Control of Special Nuclear Material
    June 1976
    U.S. NUCLEAR REGULATORY COMMISSION
    REGULATORY GUIDE
    OFFICE OF STANDARDS DEVELOPMENT
    REGULATORY GUIDE 5.57
    SHIPPING AND RECEIVING CONTROL OF
    SPECIAL NUCLEAR MATERIAL
A. INTRODUCTION
    Section 70.58 of 10 CFR Part 70, "Special Nuclear Material,"
    requires certain licensees authorized to possess at any one time and
    location special nuclear material (SNM) in quantities exceeding one
    effective kilogram to establish, maintain, and follow detailed
    fundamental material control and accounting procedures for shipping and
    receiving SNM.
    The requirements for packaging and transporting SNM are specified
    in 10 CFR Part 71, "Packaging of Radioactive Material for Transport and
    Transportation of Radioactive Material Under Certain Conditions," and in
    the applicable portions of the regulations appropriate to the mode of
    transportation in 49 CFR Parts 170-189, 14 CFR Part 103, and 46 CFR Part
    146. These requirements are not included in the scope of this guide.
    Requirements for the physical protection of SNM at licensee
    facilities and of material in transit are specified in 10 CFR Part 73,
    "Physical Protection of Plants and Materials," and are the subject of
    various regulatory guides issued or under development. Section 73.30 of
    Part 73 requires that uranium-235 (contained in uranium enriched to 20
    percent or more in the U-235 isotope), uranium-233, plutonium, or any
    combination of these materials which is 5,000 grams or more computed by
    the formula, grams = (grams contained U-235) + 2.5 (grams U-233 + grams
    plutonium), shall be shipped in containers that are sealed by
    tamper-indicating seals.(1) Licensees who transfer and receive SNM are required under section
    70.54 to complete Form NRC/ERDA-741, "Nuclear Material Transaction
    Report," and submit a copy to NRC. In addition, paragraph (c) of
    section 70.42 requires that, before transferring SNM, the person making
    the shipment verify that the recipient is authorized to receive the
    type, form, and quantity of SNM to be transferred. Paragraph (d) of
    section 70.42 outlines the methods to be used to make this verification.
    Further, by mutual arrangement with the carrier and the receiver, the
    shipper is required by paragraph (b) of section 73.30 to arrange for the
    delivery of the SNM to the receiver's facility at a time when trained
    personnel are available to properly handle the material received, and
    under section 73.36 the shipper and receiver are required to follow
    certain notification procedures.
    ----------
    (1) Regulatory Guide 5.15, "Security Seals for the Protection and
    Control of Special Nuclear Material," identifies features of security
    seal systems and describes the types of tamper-indicating seals that are
    acceptable to the NRC staff for tamper-safing SNM.
    ----------
    Section 70.57 and paragraph (f) of section 70.58 require that the
    licensee's measurement and control program for SNM must include a means
    for the control and evaluation of measurement bias and systematic and
    random errors for all parts of the measurement process, including
    scales, balances, volume measurements, analytical quality control, and
    sampling.
    Paragraph (g)(2) of section 70.58 requires that procedures be
    established to review and evaluate shipper-receiver differences on an
    individual container or lot basis, a shipment basis, and a cumulative
    basis for shipments of like material. Guidelines for performing the
    evaluation and resolution of shipper-receiver differences are contained
    in various other regulatory guides that have been issued or are under
    development;(2) these guidelines are not included in the scope of this
    guide. Any loss of SNM (other than normal operating loss) must, under
    section 70.52, be reported to the Director of the appropriate NRC
    Inspection and Enforcement Regional Office (listed in Appendix A of Part
    73) by telephone, telegram, or teletype.
    This guide describes procedures acceptable to the NRC staff for
    complying with the Commission's regulations regarding the control of SNM
    during shipment and receipt by a licensee.
B. DISCUSSION
    Adequate control of SNM during transfer between licensees includes
    (1) physical protection of the material at the licensees' facilities and
    while in transit and (2) the timely, accurate, and independent
    identification and measurement of the SNM by both shipper and receiver
    to determine and evaluate any shipper-receiver differences. These
    measurements are necessary to (1) detect the loss or theft of SNM being
    transferred between licensees, (2) detect and permit correction of
    clerical or handling errors, (3) detect falsification or errors in the
    shipment source data, (4) provide assurance that measurement bias is
    detected and corrected, and (5) detect and prevent the transfer of
    "material unaccounted for" (MUF) from one licensee to another.
    ----------
    (2) Regulatory Guide 5.28, "Evaluation of Shipper-Receiver
    Differences in the Transfer of Special Nuclear Materials," is currently
    available. A regulatory guide on the reconciliation of statistically
    significant shipper-receiver differences is under development.
    ----------
    Where tamper-indicating seals are used, their application to each
    item or container by the shipper immediately after sampling or assay and
    the prompt verification of these seals by the receiver can be help
    ensure the integrity of the material measured.
    Initial receiving checks, made immediately after receipt, can
    determine if loss, theft, or substitution of SNM may have occurred
    during transfer and can detect packaging and clerical errors. The
    checks can include counting the pieces; identifying and weighing the
    containers or items received; comparing the results with the same
    information on a bill of lading, Form NRC/ERDA-741 (Nuclear Material
    Transaction Report), or other appropriate document supplied by the
    shipper; and, to the extent possible, performing an overcheck of each
    container by nondestructive analysis or equivalent means to provide a
    gross verification of the SNM content.
    After these initial checks have been made, prompt quantitative
    verification of the contents of each container will provide early
    assurance that the contents of the packages received are identical to
    those shipped. Written procedures that call for performing these
    verifications within specific time limits after shipment can help ensure
    that Form NRC/ERDA-741 is filed in a timely fashion. In addition, the
    validity of both the shipper and receiver measurements is dependent on
    the existence of a program of standardization and calibration of
    measurement equipment and procedures.
    Prior coordination between the carrier and receiver can ensure
    that SNM will be delivered to the receiver's facility at a time when
    trained personnel are available to properly handle the material
    received. This procedure will eliminate the possibility of material
    arriving during off hours when proper receiving checks or adequate
    physical security for the material cannot be ensured.
    Appropriate procedures that identify employees who are authorized
    to ship SNM and the responsibilities of the various organizational
    components that have cognizance of the shipment will ensure that all
    aspects of the shipment are adequately coordinated. The following
    organizational components are listed with typical responsibilities as
    related to the shipment:
1. Organizational component that fabricates or assembles material:
    a. Determine the correct weights of the SNM,
    b. Obtain appropriate analysis of the SNM,
    c. Ensure product specifications,
    d. Provide guidance as to packaging or package material
    properly as required.
2. Shipping control:
    a. Prepare shipping forms,
    b. Arrange transfer of material to shipping area,
    c. Ensure proper packaging.
3. Security:
    a. Accompany package to shipping area when appropriate,
    b. Be cognizant of the storage areas while shipment is in them,
    c. Guard shipment while it is being loaded,
    d. Plan and arrange with the dispatcher of the material,
    e. Obtain signed receipts and pass them on to the appropriate
    departments.
4. Traffic (dispatcher):
    a. Make carrier arrangements,
    b. Coordinate shipments,
    c. Prepare bill of lading and other formal shipping papers,
    d. Notify receivers as to when shipments will be made and
    approximate time of scheduled arrival.
5. Nuclear materials control:
    a. Approve all SNM shipping memos,
    b. Prepare and transmit NRC/ERDA-741 forms,
    c. Transmit information for computer records, if used,
    d. Post shipping transactions to control records,
    e. Investigate and correct shipppr-receiver differences.
    To document the transfer of SNM containing 1 gram or more of
    contained uranium-235, uranium-233, or plutonium, Form NRC/ERDA-741 is
    initiated and distributed by the shipper promptly after the material is
    shipped. Normally, the licensee receiving SNM is required to measure
    independently its element and isotopic content and complete and
    distribute Form NRC/ERDA-741 within 10 days of receipt of the material.
    However, if receipt measurements cannot be completed within 10 days, a
    licensee may, when authorized by his license, prepare and distribute
    Form NRC/ERDA-284, "Nuclear Material Transfer Report," or use Form
    NRC/ERDA-741 as a temporary receipt record after performing an initial
    receiving check to verify that the items, containers, and gross
    quantities shipped have been received. In such cases, the receiver is
    then required to complete his measurements and report them on Form
    NRC/ERDA-741 within 30 days of receipt of the shipment. If the material
    received is scrap or irradiated material that may take longer than 30
    days to measure, Form NRC/ERDA-741 is completed and distributed to
    indicate temporary acceptance of the shipper's values; at a later date,
    the receiver prepares and distributes a "corrected copy" of Form
    RC/ERDA-741 that reports the receiver's own measurements.(3)C. REGULATORY POSITION
    The following methods are acceptable to the NRC staff for the
    control of shipments and receipts of special nuclear material:
1. Shipping
    a. Before shipping SNM, a licensee should ensure that the
    intended receiver is authorized to receive the type, form, and quantity
    of SNM to be transferred.
    b. The element and isotopic content of the material to be
    shipped should be measured and associated limits of error determined by
    a method whose validity is ensured by an ongoing quality control
    program.
    c. The shipper should establish and maintain written procedures
    that identify employees who are authorized to initiate shipment of SNM
    and identify the responsibilities of the various departments that should
    have cognizance of the shipment.
    d. When shipments are required to be transported in containers
    that are sealed by tamper-indicating seals, the shipper should seal all
    containers or items with the tamper-indicating device immediately after
    sampling or assaying to ensure the integrity of the material measure.
    ----------
    (3) See Section 70.54 of 10 CFR Part 70 and the written
    instructions entitled "Instructions to NRC and Agreement State Licensees
    for Reporting Nuclear Material Transfers on Form NRC/ERDA-741 - Nuclear
    Material Transaction Report," U.S. Nuclear Regulatory Commission, July
    1976. Copies of the letter may be obtained from the Division of
    Safeguards, Office of Nuclear Materials Safety and Safeguards, U.S.
    Nuclear Regulatory Commission, Washington, D.C. 20555.
    ----------
    e. Written procedures should be established and maintained to
    assign specific organizational components responsibility for packaging
    the shipment and ensuring that it is packaged and transported in
    accordance with the provisions of 10 CFR Part 71 and other applicable
    regulations.
    f. Organizational components responsible for the shipment
    within the plant and in transit should have a set of written procedures
    that cover both normal and emergency conditions.
    g. Under section 73.36(c)(1) the shipper is required to notify
    the consignee of the pertinent details of the shipment. The
    notification should include the time and method of shipping, the name of
    the carrier, and the estimated time of arrival at the receiver's
    facility. In addition, the shipper should notify the receiver of the
    bill of lading number, the seal numbers, the gross and net weights, and
    the element and isotopic content of each item or container.
    h. The shipper should initiate and distribute a Nuclear
    Material Transaction Report (Form NRC/ERDA-741) in accordance with the
    printed instructions on the form.
2. Receipts
    a. A licensee should accept receipt of only those types and
    quantities of SNM authorized by his licensee. If other material is
    delivered to his facility, the licensee should notify the shipper
    immediately so that appropriate arrangements can be made for the
    disposition of the material and the continuous maintenance of adequate
    physical protection.
    b. Arrangements should be made to deliver the material to the
    receiver at a time when he has personnel available to properly handle
    the material. If the shipment fails to arrive at the scheduled time,
    the receiving licensee is required under section 73.36(e) to notify the
    shipper so that a prompt investigation can be initiated.
    c. As soon as possible, but in no case more than 24 hours after
    receipt, the identification and integrity of the shipper's tamper-safing
    devices on each item or container should be verified. The piece count
    and identification and gross weight of the items or containers received
    should be checked against the bill of lading, Form NRC/ERDA-741, or
    other appropriate shipping document to provide assurance that the
    shipment was received intact. To the extent possible, an overcheck
    determination by nondestructive analysis (NDA) or other appropriate
    means should be made to provide a prompt estimate of the SNM content of
    each item or container. After the initial receiving checks have been
    performed, the material should be sent to an area where the contents of
    the containers or items can be verified quantitatively. Written
    procedures should be established and maintained for verifying the
    receipts within specific time limits so that Form NRC/ERDA-741 can be
    filed within the required time.
    d. If any of the tamper-safing devices have been disturbed in a
    way that may indicate an attempt to render the device inoperable or if
    the device has been accidentally damaged, the following actions should
    be taken:
    (1) The affected containers should immediately be resealed
    with another tamper-safing device, and the resealing should be witnessed
    and attested to by the personnel delivering the containers.
    (2) The containers should be weighed and a determination
    made as to whether any of the contents have been removed.
    (3) If the contents of the containers appear to be in
    order, the shipper should be notified and given the option of witnessing
    a quantitative assessment of the containers' contents within 48 hours
    following receipt of the shipment. If the shipper does not respond to
    this offer, the contents of the container should be assessed as soon as
    possible but in no case later than 48 hours after receipt.
    (4) If the contents of the containers appear to have been
    removed, the shipper and the Director of the appropriate NRC Inspection
    and Enforcement Regional Office listed in Appendix A of 10 CFR Part 73
    should be notified and given the option of witnessing a quantitative
    assessment of the containers' contents within 24 hours following
    receipt. If neither responds to this offer, the contents of the
    container should be quantitatively assessed immediately and witnessed
    and attested to by personnel from at least two different groups within
    the receiver's organization.
    e. Within the time specified in the instructions for the
    preparation of Form NRC/ERDA-741, the receiver should make an accurate,
    precise, and independent measurement of the SNM content of the material
    received. This measurement should be in accordance with a program for
    acceptable measurement quality as required by paragraph (e) of section
    70.58.
    f. The difference between the amount of SNM stated by the
    shipper as having been shipped and the amount received as measured by
    the receiver should be reviewed and evaluated.
    All measurement discrepancies should be reported to the
    nuclear material control managers or their alternates, who should
    personally verify the discrepancy in the presence of the employee who
    discovered them. Written procedures should quantitatively define what
    constitutes a discrepancy for each type of SNM received. Appropriate
    action should be taken to reconcile those shipper-receiver differences
    that are statistically significant at the 95% confidence level, except
    for shipments that involve differences of 50 grams or less of U-235 or
    plutonium. When a discrepancy is identified, the nuclear material
    manager should resolve the discrepancy with the shipper. If the
    discrepancy cannot be resolved, the appropriate NRC Inspection and
    Enforcement Regional Office should be notified by telephone, telegram,
    or teletype.
    g. Within 10 days of receipt of material, the receiver should
    complete and distribute the Form NRC/ERDA-741 prepared by the shipper.
    When receipt measurements cannot be completed within this 10-day period,
    the receiver should complete a temporary receipt in one of the following
    two ways: (1) as indicated in the instructions(3) for reporting nuclear
    material transfers on Form NRC/ERDA-741, complete blocks 17A and 17B of
    the form, note on the form whether the containers, boxes, cases, etc.,
    reported as shipped were received, and mark on the form: "Nuclear
    Material Transfer Receipt" or (2) if authorized in the license, prepare
    Form NRC/ERDA-284, "Nuclear Material Transfer Report," as a temporary
    receipt. In either case, a copy of the original Form NRC/ERDA-741
    issued by the shipper should then be completed and distributed within 30
    days of receipt to show the receiver's measurements. However, if
    measurements of scrap and irradiated material cannot be completed and
    reported within 30 days of receipt of material and if a temporary
    receipt has been filed on a Form NRC/ERDA-284 or Form NRC/ERDA-741, the
    licensee should complete Form NRC/ERDA-741 accepting the shipper's
    weights and file a corrected copy to report his own measurements at a
    later date.
D. IMPLEMENTATION
    This section provides information to applicants and licensees
    regarding the NRC staff's plans for using this regulatory guide.
    This guide consists of a compilation of practices that are
    currently in use and are acceptable to the NRC staff. Therefore, except
    in those cases in which the applicant or licensee proposes an acceptable
    alternative method, the staff will use the method described herein in
    evaluating an individual's capability for and performance in complying
    with specified portions of the Commission's regulations until this guide
    is revised as a result of suggestions from the public or additional
    staff review.
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